Das Beispiel ist nicht wirklich minimal, aber es läuft. (Ich hab bei so langen Materialangaben naturgemäss Verständnis für Naturwissenschaftler
Allerdings hatte ich keine Lust, es einzudampfen, daher habe ich nur die Änderungen eingebaut.
Zum Problem: Ich verwende gerne tabularx mit dem Paket ltablex, dann kann die Tabelle nämlich umbrochen werden.
- \nopagebreak[...] nach Überschriften, damit die Überschrift nicht allein auf einer Seite hängt. Du kannst dir auch überlegen, die nicht in die Tabelle zu packen sondern als \minisec{} o.ä. zu schreiben.
Was du noch machen solltest: Wenn du schon SIunits verwendest, dann schreib doch die Einheiten auch schön. Momentan sind sie als Zahl Leerzeichen Einheit geschrieben. Entweder SIunits nehmen, oder "1\,cm", also mit halbem Leerzeichen schreiben. So wird dann auch Zahl und Einheit nicht getrennt (bei normalem Leerzeichen Tilde verwenden).
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\chapter{Introduction}
\chapter{Experiments}
\section{material and hardware}
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\begin{tabularx}{\textwidth}{@{}p{6cm}X}
\textbf{Material}& \\\nopagebreak[4]
Blood collection tube&4 x 7.5 ml Plasma Lithium-Heparin S-Monovette tubes\newline Sarstedt, Nümbrecht, Germany\\
C18 Purification&ZipTip Pipette Tips\newline Millipore, Billerica, MA, USA\\
Disposables&Greiner Bio-One GmbH, Frickenhausen, Germany\newline Eppendorf, Hamburg, Germany\newline Beckman Coulter, Brea, CA, USA\\
Filter&Ultrafree-MC (Durapore, 0.65 \micro m)\newline Millipore, Billerica, MA, USA\\
Microspheres & Carboxylated Mikrospheres\newline Luminex, Austin, TX USA\\
MALDI Targets&Prespotted Anchor Chips \newline Bruker Daltonik GmbH, Bremen, Germany\\
Magnetic microspheres & Dynabeads Protein G\newline Invitrogen, Carlsbad, CA, USA\\
Mikrotiter Filterplates & 1.2 \micro m Durapore PVDF\newline Millipore, Billerica, MA, USA\\
PCR-Plates & KingFisher 96 KF plate (200 \micro l)\newline ThermoFisher Scientific,Waltham, MA, USA \\
PCR tip comb & KingFisher 96 tip comb for PCR magnets\newline ThermoFisher Scientific,Waltham, MA, USA\\
Single use cuvettes & UVette\newline Eppendorf, Hamburg, Germany\\
Syringe Filter&Rotilabo, sterile (0.22 \micro m PES)\newline Carl Roth, Karlsruhe, Germany\\
Syringe needles&19-gauge 100 Sterican\newline B. Braun Melsungen AG, Melsungen, Germany\newline 21-gauge Safety Multifly 0.8 mm / 19mm needle\newline Sarstedt, Nümbrecht, Germany\\
\\
\textbf{Hardware} & \\\nopagebreak[4]
Balances&Explorer E12140 \newline OHAUS, Pine Brook, NJ, USA\newline MC1 Research RC210\newline Sartorius AG, Göttingen, Germany\\
Bead based array analyzer& Luminex 100/200\newline Luminex, Austin, TX USA\\
Centrifuges&Hettich Rotanta/RPC RP5094 rotor \newline Hettich Lab technology, Tuttlingen, Germany \newline 5415D und 5810R\newline Eppendorf, Hamburg, Germany\\
Chromatography Systems&ÄKTAxpress\newline GE Healthcare Bio-Sciences AB, Uppsala, Sweden\\
Geldocumentation&Kodak Image Station 440 CF\newline Kodak Eastman, Rochester, NY, USA\\
Mass spectrometer& MALDI-TOF/TOF Ultraflex III\newline Bruker Daltonik, Bremen, Germany\newline 6410 Triple Quadrupole LC/MS\newline Agilent Technologies, Santa Clara, CA, USA\\
Magnets&Invitrogen, Carlsbad, CA, USA\\
Magnetic bead handler&Thermo Scientific KingFisher® Flex and KingFisher 96®\newline ThermoFisher Scientific,Waltham, MA, USA \\
Orbital shaker&KL-2\newline Edmund Bühler GmbH, Hechingen, Germany\\
pH meter&pH meter 766\newline Knick, Berlin, Germany\\
Photometer&BioPhotometer plus\newline Eppendorf, Hamburg, Germany\\
Pipettes&Eppendorf, Hamburg, Germany\\
SDS PAGE System&XCell Sure Lock Mini Cell, Power Ease 500\newline Invitrogen, Carlsbad, CA, USA\\
Shaker&Vortex Genie 2\newline Scientific Industries, Bohemia, NY, USA\\
Syringe pump&Model 22\newline Harvard Apparatus, Holliston, MA, USA\\
Thermomixer&Thermomixer comfort\newline Eppendorf, Hamburg, Germany\\
Swivel roller mixer&RM5\newline Assistent, Sondheim, Germany\\
Ultra pure water system&Arium 61316/611VF\newline Sartorius, Göttingen, Germany\\
Ultracentrifuge&TL-100\newline Beckman Coulter, Brea, CA, USA\\
Ultrasonic bath&RK 31\newline Bandelin, Berlin, Germany\\
\\
\textbf{Software}& \\\nopagebreak[4]
Data Collection Bead based arrays&Exponent 3.1 Luminex, Austin, TX, USA\\
Data Collection Mass spec&FlexControl 3.0\\
Data Evaluation Mass spec&FlexAnalysis 3.0, Biotools 3.1\\
&Bruker Daltonik GmbH\\
\end{tabularx}
\section{Reagents and chemicals}
\begin{tabularx}{\textwidth}{@{}p{6cm}X}
\textbf{Antigen Generation}& \\\nopagebreak[4]
DMSO&Fluka (Sigma-Aldrich)\newline St. Louis, MO, USA\\
KLH&Pierce (Thermo Fisher Scientific)\newline Waltham, MA, USA\\
Sodiumazide&Merck KGaA\newline Darmstadt, Germany\\
PBS&PAA Laboratories GMbH\newline Pasching, Austria\\
sulfo-MBS&Pierce (Thermo Fisher Scientific)\newline Waltham, MA, USA\\
Peptides&Intavis AG\newline Reutlingen, Germany\\
TCEP&Fluka (Sigma-Aldrich)\newline St. Louis, MO, USA\\
\\
\textbf{Microsphere based Microarrays}& \\\nopagebreak[4]
Acetonitrile&Merck KGaA\newline Darmstadt, Germany\\
BSA (Albumin Fraction V\newline Protease-free)&Carl Roth\newline Karlsruhe, Germany\\
Blocking Reagent& Roche\newline Mannheim, Germany\\
Di-Sodiumhydrogenphosphate&Fluka (Sigma-Aldrich)\newline St. Louis, MO, USA\\
EDC&Pierce (Thermo Fisher Scientific)\newline Waltham, MA, USA\\
Donkey anti rabbit phycoerythrin&Jackson Immunoresearch\newline West Grove PA, USA\\
%Donkey anti rat phycoerythrin&Jackson Immunoresearch West Grove, PA, USA\\
Donkey anti sheep phycoerythrin&Jackson Immunoresearch\newline West Grove, PA, USA\\
Goat anti mouse phycoerythrin&Jackson Immunoresearch\newline West Grove, PA, USA\\
Mouse anti cmyc&Clone 9E10, Institute for molecular immunology\newline Helmholtzzentrum, Munich, Germany\\
MES&Sigma-Aldrich\newline St. Louis, MO, USA\\
Rat anti HA&Clone 3F10, Institute for molecular immunology\newline Helmholtzzentrum, Munich, Germany\\
Streptavidin&Pierce, Bonn, Germany\\
Streptavidin-Phycoerythrin&Jackson Immunoresearch\newline West Grove, PA, USA\\
Sulfo-NHS&Pierce (Thermo Fisher Scientific)\newline Waltham, MA, USA\\
Sulfo-SMPB&Pierce (Thermo Fisher Scientific)\newline Waltham, MA, USA\\
Tween20&Merck KGaA\newline Darmstadt, Germany\\
Activation buffer&100 mM Sodiumhydrogenphosphate, pH 6.2\\
Blocking buffer&Blocking Reagent (Roche)\newline solved in H$_2$O$_{dd}$ + 0.05\% (v/v) Tween20\\
Coupling buffer&50 mM MES, pH 5.0\\
Stock solution&10 mg/ml BSA in PBS\\
Washing buffer Luminex &0.05\% (v/v) Tween20 in PBS\\
\\
\textbf{Antibody Purification}& \\\nopagebreak[4]
Ammoniumacetate&Merck KGaA\newline Darmstadt, Germany\\
Citrate&Sigma-Aldrich\newline St. Louis, MO, USA\\
Ethanolamine&Carl Roth\newline Karlsruhe, Germany\\
Maleimide activated BSA (SMCC)&Pierce (Thermo Fisher Scientific)\newline Waltham, MA, USA\\
Sodium chloride&Carl Roth\newline Karlsruhe, Germany\\
Hydrochloride acid&Carl Roth\newline Karlsruhe, Germany\\
Activation buffer&1 mM HyHydrochloride acid\\
Binding buffer&PBS\\
Deactivation buffer I&0.5 M Ethanolamine, 0.5 M Sodium chloride, pH 8.3\\
Deactivation buffer II&0.1 M acetate, 0.5 M Sodium chloride, pH 4.0\\
Elutionbuffer Antibody Purification &0.1 M Citrate, pH 2.5\\
\\
\multicolumn{2}{@{}l}{\textbf{Immunoaffinity Chromatography}} \\\nopagebreak[4]
Ammoniumbicarbonate&Fluka (Sigma-Aldrich)\newline St. Louis, MO, USA\\
Ammoniumphosphate&Sigma-Aldrich\newline St. Louis, MO, USA\\
PBS&PAA Laboratories GMbH\newline Pasching, Austria\\
Dimethyl Pimelimidate dihydrochloride&Sigma-Aldrich\newline St. Louis, MO, USA\\
Formic acid&Biosolve\newline Valkenswaard, Netherlands\\
n-Octyl-ß-D-glucopyranosid&Applichem\newline Darmstadt, Germany\\
Triethanolamine&Carl Roth\newline Karlsruhe, Germany\\
Trifluoro acetic acid&Biosolve\newline Valkenswaard, Netherlands\\
Stopping solution&150 mM Ethanolamin, pH 9.0\\
Elutionbuffer TXP& 0.1 \% Formic acid\\
Washing buffer PBSN&PBS + 0.3\% n-Octyl-ß-D-glucopyranosid\\
Washing buffer ABCN&50 mM Ammoniumbicarbonate pH 7.4 \newline + 0.3\% n-Octyl-ß-D-glucopyranosid\\
\\
\multicolumn{2}{@{}l}{\textbf{C18 Chromatography using ZipTip Pipette Tips}} \\\nopagebreak[4]
Wetting solution&100\% Acetonitrile\\
Equilibration solution&0.1\% TFA\\
Washingbuffer ZipTip&0.1\% TFA + 5 \% Methanol\\
Elution buffer ZipTip&80\% Acetonitrile + 0.1\% TFA\\
\\
\textbf{Plasma Digest}& \\\nopagebreak[4]
Acetic Acid&Biosolve\newline Valkenswaard, Netherlands\\
Ammoniumphosphate&Sigma-Aldrich\newline St. Louis, MO, USA\\
Iodoacetamide&Sigma-Aldrich\newline St. Louis, MO, USA\\
Phenylmethylsulfonylfluorid&Roche Diagnostics\newline Mannheim, Germany\\
Tris(2-carboxyethyl)phosphine&Sigma-Aldrich\newline St. Louis, MO, USA\\
Trypsin&Sigma-Aldrich\newline St. Louis, MO, USA\\
Trypsin Gold&Promega\newline Madison, WI, USA\\
\\
\textbf{MALDI MS}& \\\nopagebreak[4]
Washing Buffer MS &10 mM Ammoniumphosphate + 0.1\% TFA\\
\\
\textbf{Ultracentrifugation}& \\\nopagebreak[4]
Goat anti Human IgG Cy3&Dianova\newline Hamburg, Germany\\
Goat anti Human IgG Cy5&Dianova\newline Hamburg, Germany\\
Sucrose&Sigma-Aldrich\newline St. Louis, MO, USA\\
\\
\textbf{SDS PAGE}& \\\nopagebreak[4]
Antioxidants&NUPage Antioxidant\newline Ivitrogen, Carlsbad, CA, USA\\
Runningbuffer&NuPage SDS MES or MOPS Runningbuffer\newline Ivitrogen, Carlsbad, CA, USA\\
Samplebuffer&NuPage LDS Samplebuffer\newline Ivitrogen, Carlsbad, CA, USA\\
Protein Standard&SeeBlue Plus2 Pre-Stained Standard\newline Ivitrogen, Carlsbad, CA, USA\\
Reducing Agent&NuPage Sample Reducing Agent\newline Ivitrogen, Carlsbad, CA, USA\\
Coomassie Solution&0.2\% (w/v) Coomassie Brilliant Blue, 50\% methanol,\\ 10\% acetic acid\\
Destaining Solution I&50\% ethanol, 10\% acetic acid\\
Destaining Solution II&10\% ethanol, 5\% acetic acid\\
\end{tabularx}
\end{document}
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